KDR Assisted Deposit ReadMe form User agreement Before we can deposit your data, you must confirm, by ticking each circle, that: X You have an ORCiD affiliated with the University of Kent; X You have prepared your data and it meets FAIR data standards; X You have selected a licence for your data reuse; Information about your data Title: [FeII(R-trz)3]·A2 accelerated aging time-lapse videos Keep this short and relevant. Do not use a title the same as that of a publication. Do not start it with the word ‘data’. Creators: At least one Kent person with a Kent email. Add as many lines as you need. Full name Rhona Lonergan Full email address rl414@kent.ac.uk Institution University of Kent ORCiD 0000-0002-9157-1604 Full name Full email address Institution ORCiD Contact email : rhonalonergan.96@gmail.com An alternative address for someone associated with the data that will be valid in the long term. eg. your personal non-Kent address Divisions: School of Chemistry and Forensic Science The University of Kent department with which this data collection should be associated. Source of funding that supported the data collection. Leverhulme Trust Related works List any theses, publications or other data sets related to this data Name and location/Reference of the related work: Spontaneous Synthesis of [FeII(Atrz)3]SO4 and its Analogues Through Accelerated Ageing: New Insights from Small-Scale Reactions Full URL https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/chem.202201823 Name and location/Reference of the related work: Developing non-traditional methods for the design, synthesis, and analysis of spin crossover materials Full URL https://kar.kent.ac.uk/113726/ DOI : If the data has been archived elsewhere and has a DOI, please include it here. If not, one will be created for you. Type of data: Please select, with a tick in the circle, an appropriate data type. If a suitable category is not listed, select 'Other'. o Dataset: Data encoded in a defined structure o Collection: A collection of samples, or various files of different data types o Image: Digitised or born digital still images, drawings or photographs X Audiovisual: Films or video. May include sound. o Software: A computer programme in source code or compiled form supporting scholarly research. o Text: Grey literature, lab notes, accompanying materials, data management plan, conference poster o Workflow: A structured series of steps which can be executed to produce a final outcome (A methodology). o Other: Description: If you selected Other above then describe the data here. Collection period: The time period for generation of the data, e.g. dates of fieldwork, length of project, exhibition running time. From: 2020/01/20 To: 2024/08/01 Geographic location of data collected: Canterbury, UK Original data publication details: If the data is archived elsewhere, please give details, including a URL. Compulsory if a data file is not uploaded Original data publisher: The name of the repository or archive Original data publication URL: Original publication date:(yyyy/mm/dd) Files to upload Include this information for each file you send to us and add rows as needed. Appendix i -Chapter 3 AA videos Video 1 (V1) – GIF of the single-crystal-scale synthesis of 1, over 42 minutes at ambient RH. Video 2 (V2) – GIF of the bulk-scale synthesis of 1, over 90 minutes at 99% RH. Video 3 (V3) – GIF of the single-crystal-scale synthesis of 1b, over 90 minutes at ambient RH. Video 4 (V4) – GIF of the bulk-scale synthesis of 1b, over 180 minutes at 99% RH. Video 5 (V5) – GIF of the single-crystal-scale synthesis of 2, over 98 minutes at ambient RH. Video 6 (V6) – GIF of the repeat single-crystal-scale synthesis of 2, over 180 minutes at 99% RH Video 7 (V7) – GIF of the bulk-scale synthesis of 2, over 6 hours at 99% RH. Video 8 (V8) – GIF of the single-crystal-scale synthesis of 3, over 29 minutes at ambient RH. Video 9 (V9) - GIF of the bulk-scale synthesis of 3, over 56 minutes at 99% RH. Video 10 (V10) - GIF of the single-crystal-scale synthesis of 4, over 150 minutes at 99% RH. Video 11 (V11) – GIF of the bulk-scale synthesis of 4, over 4 hours and 40 minutes at 99% RH. Video 12 (V12) - GIF of the bulk-scale synthesis of 1 in a DCM atmosphere over 1 day. Video 13 (V13) - GIF of the bulk-scale synthesis of 2 in a DCM atmosphere over 1 day. Video 14 (V14) - GIF of the bulk-scale synthesis of 3 in a DCM atmosphere over 1 day. Video 15 (V15) - GIF of the bulk-scale synthesis of 1 in an acetone atmosphere over 1 day. Video 16 (V16) - GIF of the bulk-scale synthesis of 2 in an acetone atmosphere over 1 day. Video 17 (V17) - GIF of the bulk-scale synthesis of 3 in an acetone atmosphere over 1 day. Video 18 (V18) - GIF of the bulk-scale synthesis of 1 in an ethanol atmosphere over 1 day. Video 19 (V19) - GIF of the bulk-scale synthesis of 2 in an ethanol atmosphere over 1 day. Video 20 (V20) - GIF of the bulk-scale synthesis of 3 in an ethanol atmosphere over 1 day. Your preferred licence for these files: CC_BY Availability of this file: Immediately openly available online no Under embargo yes If under embargo, state the date the file will become openly available: 2029/01/01 Anything else Include here anything else you would like to say about your data, for instance provenance, methodology etc.